short path distillation

  • The Short Path Distillation Head Bertha 100, since development in 2018, has become one of the leading standards in distillation head types in the industry. 2023 has brought the Bertha 100 to its final perfect form with 6 generations of evolution. This head comes equipped with 45/50 thermoport, 34/45 discharge port and a 100mm bore that secures to a boiling flask with o-ring and clamp. The Short Path Distillation Head Bertha 100 (previously SPD-4 MPD Big Bertha) is an extremely high vapor fractionation column head. The first section starts in the flask to retain as much heat in the column as possible. This entire column and entry into flask is isolated from the outside air and the flange fittings. The first chamber is a rough fractionation chamber with a lower rejection section that prevents any condensate from moving upwards. The center section is a secondary refinement section and will further refine the vapors. The upper third section is our patented fraction collector. The first dual stage fractionation column to ever be invented or used in distillation glassware, pilot or small scale. Can achieve 2-4 liters per hour (6 liters per hour with upgraded chilling and vacuum accessories) first pass and ready for crystallization. Vigs are not needed for this technology due to the industry first "no-vig" approach which utilizes a baffled section that extends down below the head base and into the boiling flask. Requirement to use these heads would be a sogevac + dual e2m30 -or- sogevac + e80 -or-  sogevac + e80 + diffusion array. This particular setup benefits from a custom diffusion array and an Apollo Vacuum Controller with the inert gas sweeping feature. Effectively increasing the stock speed and lowering the temperatures further. Included: Our flanged heads fit exclusively to Summit MPD boiling flasks: Refer to our instructional (SPD-4 MPD Complete) for correct setup of this head. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process.       Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Short Path Distillation Head Bertha 100
  • The Sensor Ultra Sensitive features the brand new, ultra-sensitive sensor. This package is unique in that - not only does it serve distillation and extraction processes - but also serves Chromatography, Conversion Reaction, and other processes that require more extreme detection. For certain processes, highly sensitive process monitoring is essential. Generally speaking, the more solvent involved in the process means the more sensitive the sensor needs to be. With that in mind, the ULTRA was created. If you are an existing customer, you have the option to upgrade to a standalone ULTRA Sensor for $1,350. Please call us for more details. Use this sensor on any chromatography column with the GL18 to #34 adapter. The Fraction Finder Sensor 34/45 consists of an optical light pulse and detector, acting as “the eyes” of the system. It wraps around a distillation/chromatography setup tube and connects to the Fraction Finder display to track important data on the process.
    • Fraction Finder optical sensor with ultra-sensitive detector
    • Magnetic locking mechanism
    • Anodized aluminum apertures
    • 90° strap rotation
    • Currently only available in size 34mm
    • Validated by Arometrix for use on distillation systems
    • Currently being tested on reverse-phase chromatography processes
    • Display and sight glass not included

    Information common with all Fraction Finder sensors

    These sensors are black for a reason:
    • Black absorbs all light while blocking out ambient light.
    • This leads to better signaling and the most valid data possible transmitting to the Fraction Finder display.
    • For example, a white sensor wouldn’t work because it would reflect the light into your glassware and into the sensor, harming the reading.
    Chemical Resistant
    • This reduces any degradation from solvents, crude oils, extracts, etc..
    • This protects the sensor and ensures that it lives to see an endless amount of runs.
    Thermo Resistant / Safety
    • The black coating we use on each sensor is a high temperature, thermal resistant coating, it can withstand temperatures well above anything you’d see in a distillation lab.
    • It’s nearly impossible to set one of our sensors on fire, the coating is almost completely fireproof!
    • This protects the user, the equipment, and (in worst case scenarios) the entire lab.
    Sensor only, monitor and accessories not included.
  • Sensor #34

    $2,094.99
    The Fraction Finder Sensor #34 consists of an optical light pulse and detector, acting as “the eyes” of the system. It wraps around a distillation set up condenser tube and connects to the Fraction Finder display to track important data on the distillation. These sensors are black for a reason:
    • Black absorbs all light while blocking out ambient light.
    • This leads to better signaling and the most valid data possible transmitting to the Fraction Finder display.
    • For example, a white sensor wouldn’t work because it would reflect the light into your glassware and into the sensor, harming the reading.
    Chemical Resistant
    • This reduces any degradation from solvents, crude oils, extracts, etc..
    • This protects the sensor and ensures that it lives to see an endless amount of runs.
    Thermo Resistant / Safety
    • The black coating we use on each sensor is a high temperature, thermal resistant coating, it can withstand temperatures well above anything you’d see in a distillation lab.
    • It’s nearly impossible to set one of our sensors on fire, the coating is almost completely fireproof!
    • This protects the user, the equipment, and (in worst case scenarios) the entire lab.
    Sensor only, monitor and accessories not included.
  • Sensor #29

    $1,919.99
    The Fraction Finder Sensor #29 consists of an optical light pulse and detector, acting as “the eyes” of the system. It wraps around a distillation set up condenser tube and connects to the Fraction Finder display to track important data on the distillation. These sensors are black for a reason:
    • Black absorbs all light while blocking out ambient light.
    • This leads to better signaling and the most valid data possible transmitting to the Fraction Finder display.
    • For example, a white sensor wouldn’t work because it would reflect the light into your glassware and into the sensor, harming the reading.
    Chemical Resistant
    • This reduces any degradation from solvents, crude oils, extracts, etc..
    • This protects the sensor and ensures that it lives to see an endless amount of runs.
    Thermo Resistant / Safety
    • The black coating we use on each sensor is a high temperature, thermal resistant coating, it can withstand temperatures well above anything you’d see in a distillation lab.
    • It’s nearly impossible to set one of our sensors on fire, the coating is almost completely fireproof!
    • This protects the user, the equipment, and (in worst case scenarios) the entire lab.
    Sensor only, monitor and accessories not included.
  • Reflux condensers are used in “conversion” processes to cool the vapor molecules emitted from heated oils to change their gaseous state back into liquid by means of a chilled triple coil. This unit is recommended for 22L and larger boiling flasks. How it works: The condenser is attached to the boiling flask joint and is secured in a vertical position. Chiller fluid is circulated through the coil to cause the vapors to condense as they rise up through the condenser coils thus preventing them from escaping. This gives you the option to reflux different fluids in your boiling flask for extended periods of time before you run the SPD, this is a must have in the lab for conversions. Flask entry port is 55/50 with 24/40 exit port. High Temp GLs included.  24/40 to GL14 Adapter OR 24/40 to GL18 Adapter included. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve. NEED A 45/50 PORT? Call us, you can custom order anything! Base not included Summit recommends all users to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Reflux Condenser Triple Coil
  • Reflux condensers are used in “conversion” processes to cool the vapor molecules emitted from heated oils to change their gaseous state back into liquid by means of a chilled dual coil. This unit is recommended for 12L and smaller boiling flasks. How it works: The condenser is attached to the boiling flask joint and is secured in a vertical position. Chiller fluid is circulated through the coil to cause the vapors to condense as they rise up through the condenser coils thus preventing them from escaping. This gives you the option to reflux different fluids in your boiling flask for extended periods of time before you run the SPD, this is a must have in the lab for conversions. Flask entry port is 55/50 with 24/40 exit port. Total dimensions 25.75 x 2.25 inch. High Temp GLs included. 24/40 to GL14 Adapter OR 24/40 to GL18 Adapter included. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve. NEED A 34/45 PORT? Call us, you can custom order anything! Base not included Summit recommends all users to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Reflux Condenser Dual Coil
  • Raschig Rings 8x8 are small pieces of borosilicate tube used in large numbers as a packed bed within columns for distillation. These glass rings provide a large surface area within the volume of the column for interaction between liquid and gas vapors. Rings actually measure 8x10mm in size. 1 Pound bag. Also available:     Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Raschig Rings 8x8
  • Raschig Rings 6x6 are small pieces of borosilicate tube used in large numbers as a packed bed within columns for distillation. These glass rings provide a large surface area within the volume of the column for interaction between liquid and gas vapors. Rings actually measure 6x8mm in size. 1 Pound bag. Also available:     Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Raschig Rings 6x6
  • $7,373.00

    The Polyscience IP-80 Immersion Chiller has a custom condenser probe unit for cold traps. Continuous cooling to temperatures as low as -80°C. Key Features:
    • Working Temperature Range C: -40°C to -80°C
    • Designed to run at maximum cooling
    • An economical alternative to dry ice or liquid nitrogen
    • Excellent for trapping applications, freeze drying, and rapidly cooling small volumes of liquids
    • Overall Dimensions (L x W x H) 20.1 x 15 x 22.3 in
    • Refrigerant R404A & R508B
    Recommended traps:   To purchase, please contact Summit Research at 831-226-2948 or by eMail. Items ship 1-3 days after orders have been processed unless otherwise specified. Price does not include shipping and will be included in your final estimate before processing.
  • Liquid Temp Control Key 45/50 is a short path distillation head key that is used to generate a localized cold/hot surface. The temperature achieved reduces or enlarges the quantity of volatile material exhausted into the air. This premium Schott glass 45mm plug is 14.25 inch overall length and 10.5 inch from the bottom of the frosted taper with 4 large bands. High Temp GL14s included. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process.       Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Liquid Temp Control Key 45/50
  • Liquid Temp Control Key 34/45 is a short path distillation head key that is used to generate a localized cold/hot surface. The temperature achieved reduces or enlarges the quantity of volatile material exhausted into the air. This premium Schott glass 34mm plug is 8.5 inch overall length and 4.5 inch from the bottom of the frosted taper with the tip being a small condenser coil. High Temp GL14s included. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process.         Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Liquid Temp Control Key 34/45
  • Laminar Path Monocow 34 is a traditional short path distillation distribution adapter. Added condenser coil allows you to dial in the temps. 34/45 all the way through with 29 to flask and 24 to vacuum port. Laminar Path comes with 24/40 Stopper and GL14s, with choice to add a stainless steel #24/40 KF25 adapter. Glassware used for maximum efficiency distillation. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process. Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Laminar Path Monocow 34
  • Laminar Path Monocow 29 is a traditional short path distillation distribution adapter. Added condenser coil allows you to dial in the temps. 29/42 from the head and 34/45 to the cold trap. 29 to flask and 24 to vacuum port with all tapers traditional. Laminar Path comes with 24/40 Stopper and GL14s, with choice to add a stainless steel #24/40 KF25 adapter. Glassware used for maximum efficiency distillation. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process. Summit recommends all users of any and all glassware to operate inside a ventilated area with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Laminar Path Monocow 29
  • Laminar No Discharge 34 is a shorter, more compact unit which allows for higher temperatures in the vapor bypass. Coil-less laminar with less turbulence and no discharge. Comes with #24 glass stopper and choice of #24/40 KF25 adapter. Moreover, these short path distillation arms are used in conjunction with a Swing Arm Kit. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process.   Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Laminar No Discharge 34
  • Laminar No Discharge 29 is a shorter, more compact unit which allows for higher temperatures in the vapor bypass. Coil-less laminar with less turbulence and no discharge. Comes with #24 glass stopper and choice of #24/40 KF25 adapter. Moreover, these short path distillation arms are used in conjunction with a Swing Arm Kit. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process. Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Laminar No Discharge 29
  • Laminar Coiled No Discharge 34 is a shorter, more compact unit which allows for higher temperatures in the vapor bypass. Coiled laminar with less turbulence and no discharge. Comes with #24 glass stopper and choice of #24/40 KF25 adapter. Moreover, these short path distillation arms are used in conjunction with a Swing Arm Kit. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process.   Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Laminar Coiled No Discharge 34
  • Laminar Coiled No Discharge 29 is a shorter, more compact unit which allows for higher temperatures in the vapor bypass. Coiled laminar with less turbulence and no discharge. Comes with #24 glass stopper and choice of #24/40 KF25 adapter. Moreover, these short path distillation arms are used in conjunction with a Swing Arm Kit. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process.   Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Laminar Coiled No Discharge 29
  • Laminar Coil-less 34 is a shorter, more compact short path distillation arm which allows for higher temperatures in the vapor bypass. A true laminar with less turbulence. Comes with #24 glass stopper and choice of #24/40 KF25 adapter. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process.     Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Laminar Coil-less 34
  • Laminar Coil-less 29 is a shorter, more compact short path distillation arm which allows for higher temperatures in the vapor bypass. A true laminar with less turbulence. Comes with #24 glass stopper and choice of #24/40 KF25 adapter. As always, Summit uses 100% best quality glass blanks that are THICKER and built BEYOND STANDARDS made right here in the USA. Our glassware is made specifically for efficiency and durability. Summit provides the quality of lab equipment that you deserve to streamline your short path distillation process.       Summit recommends all users of any and all glassware to operate inside a ventilated fume hood with sufficient blast shields to prevent injury in case of fatigued glass failure. Summit is not responsible or liable for the result of any failures from use, and/or loss of subsequent hardware contamination/failure with or without the result of material loss or damaged caused to surroundings. By purchasing our premiere lines of laboratory glassware the user is responsible to operate in the recommended environment safely. We recommend all users to operate in a legal and licensed facility where safety is the number 1 goal. Laminar Coil-less 29
  • 100g Long term lubrication for high temperature applications under the influence of aggressive media up to 250C. Klübertemp GR RT greases are white, homogeneous long-term greases based on perfluorinated polyether oils (PFPE) and polytetrafluoroethylene (PTFE). This series contains greases with a range of specific additives for use in different applications. Klübertemp GR RT 15 shows good compatibility with plastics and elastomers, enabling a wide range of component materials to be selected. Vapor pressure of 2.0 x 10⁸ Torr at 20°C Vapor pressure of 4.7 x 10⁶ Torr at 100°C   
  • The KF40 O Ring will fit between any KF40 flange while using a KF40 clamp. Made from Viton and stainless steel.
  • The KF40 Clamp combined with KF40 O Ring form a vacuum tight seal between the connection flanges. This circumferential clamp is used for connecting standard NW40 / KF40 vacuum components. Aluminum clamp with butterfly nut for easy tightening.
  • KF40 Bellow

    From: $289.99
    The KF40 Bellow is a corrugated stainless steel pipe that connects to corresponding kf40 flanges. These malleable pipes allow for some error as apposed to hooking up a solid straight pipe. Available in 24 and 36 inch lengths. Don't forget other KF40 fittings and accessories: 100% stainless steel. 100% USA made. Bellow warning: Stretch and bend your bellow into position before installation. Engaging your pump(s) while not doing so could make the bellow jolt/jostle, putting stress on or damage glassware, voiding limited warranties. KF40 Bellow
  • Billet stainless steel adapter that reduces the diameter of your KF vacuum pipe. KF40 to KF25 flange. Summit has corresponding KF25 and KF40 products in our Stainless Steel section.
  • KF25 Tee

    $79.99
    The KF25 Tee is cut from 100% billet stainless steel. At Summit, quality is everything. Don't accept the imitations. 100% USA made.
  • KF25 Straight Pipe is an 8 inch stainless steel high vacuum pipe. KF25 Flanges. Summit has other KF25 products in our Stainless Steel section.   Looking for a specific length?.. we might be able to help! Call us
  • KF25 O Ring will fit between any KF25 flange while using a KF25 clamp. Made from Viton and stainless steel.
  • 1" Male JIC to KF25 adapter (Harvest Right Adapter) fits any KF25 flange. Summit's stainless adapters contain 100% USA made precision billet steel. Why choose an adapter with multiple parts and more chances to leak?
  • Sale!

    KF25 Cross

    Original price was: $99.99.Current price is: $42.99.
    The KF25 cross is a staple in most larger vacuum systems that require that extra flange for vacuum gages or other high vacuum devices. Built to last with 304 stainless steel and superior TIG welding. All KF flanges connect with o-ring and clamp (links below). Cross is 4 inch end to end.
  • The KF25 Clamp combined with KF25 O Ring form a vacuum tight seal between the connection flanges. This circumferential clamp is used for connecting standard NW25 / KF25 vacuum components. Aluminum clamp with butterfly nut for easy tightening.